Process for preparation of high strength polyurethane aqueous dispersion


Application Number: 00116114
Application Date: 2000.09.25
Publication Number: 1285364
Publication Date: 2001.02.28
Priority Information:
International: C08J3/03;C08L75/04
Applicant(s) Name: Sichuan Heguang High Technology Development Co., Ltd.
Address:
Inventor(s) Name: Yue Yilun;Wu Dake;Yu Hui
Patent Agency Code: 51126
Patent Agent: yang dunhua
Abstract The present method of high-strength polyurethane water dispersion includes the following steps: prepolymerization of aliphatic or aromatic diisocyanate with polyester or polyether dihydric alcohol at 40-90 deg.C in a mole ratio of 1.5-2.1:1 for 1-6hr., after prepolymerization adding vinyl monomer whose added quantity is 20-80% of total weight of said polymer as diluting agent, and adding low-molecular dihydric alcohol or diamine chain extender in a 0.5-0.9:1 mole ratio of it and residuel isocyanic acid radical to make chain extending reaction for 1-4 hr, after the chair-extending reaction cooling system temp. to 28-35 deg.C, and adding colloid stabilizing agent whose added quantity is 2-8 % of total weight of said polymer, then making water dispersion in the presence of surfactant whose added quantity is 0.5-3% of total weight of said polymer. After the emulsion is stabilized vinyl monomer polymerization is effected by conventional process.